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101.
Mass transfer rates were determined in a 3.4 cm i.d. trickle-bed reactor in the absence of reaction by absorption measurements and in presence of reaction. Gas flow rates were varied from 0-100 l/h and liquid flow rates from 0-1.5 l/h. The catalyst particles were crushed to an average diameter of 0.054 and 0.09 cm. Mass transfer coefficients remained unaffected by change in gas flow rate but increased with liquid rate. The data from absorption measurements were evaluated with predictions based upon plug-flow and axial dispersion model. Mass transfer coefficients were found greater in case of axial dispersion model than that of plug-flow model specially at low Reynolds number (Re1 < 1).Hydrogenation of α-methylstyrene to cumene using a Pd/Al2O3 catalyst was taken as a model reaction. Intrinsic kinetic studies were made in a laboratory-stirred-autoclave. Mass transfer coefficients were determined using these intrinsic kinetic data from the process kinetic measurements in trickle-bed reactor. Mass transfer coefficients under reaction conditions were found to be considerably higher than those obtained by absorption measurements.Correlations were suggested for predicting mass transfer coefficients at low Reynolds number.The gas to liquid mass transfer coefficients for lower gas and liquid flow rates were determined in a laboratory trickle-bed reactor. The effect of axial dispersion on mass transfer was considered in order to evaluate the experimental data. Three correlations were formulated to calculate the mass transfer coefficients, which included the effect of liquid loading, particle size and the properties of the reacting substances. The gas flow rate influences the gas to liquid mass transfer only in the region of low gas velocities. In the additional investigations of gas to liquid mass transfer without reaction in trickle-bed reactor, the mass transfer coefficients were determined under reaction conditions and the intrinsic kinetics was studied in a laboratory scale stirred autoclave with suspended catalyst. A few correlations are formulated for the mass transfer coefficients. A comparison with the gas-liquid mass transfer coefficient obtained by absorption measurements showed considerable deviations, which were illustrated phenomenologically. 相似文献
102.
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104.
Data replication techniques are used in data grid to reduce makespan, storage consumption, access latency and network bandwidth. Data replication enhances data availability and thereby increases the system reliability. There are two steps involved in data replication, namely, replica placement and replica selection. Replica placement involves identifying the best possible node to duplicate data based on network latency and user request. Replica selection involves selecting the best replica location to access the data for job execution in the data grid. Various replica placement and selection algorithms are available in the literature. These algorithms measure and analyze different parameters such as bandwidth consumption, access cost, scalability, execution time, storage consumption and makespan. In this paper, various replica placement and selection strategies along with their merits and demerits are discussed. This paper also analyses the performance of various strategies with respect to the parameters mentioned above. In particular, this paper focuses on the dynamic replica placement and selection strategies in the data grid environment. 相似文献
105.
A systematic strategy is developed for the location of the source and the rectification of gross, biased measurement errors in a chemical process. The proposed strategy proceeds in three levels: (a) A structural analysis of the balance equations identifies subsets of balances with measurements which are suspected to possess gross errors. (b) A sequential analysis of the balance equations with suspect measurements further reduces the size of the problem. Statistical criteria are used in this step. (c) Finally, a sequential analysis of the suspect measurements appearing in the reduced set of balances leads to the identification of the source of the gross errors.The proposed strategy: (i) reduces the size of the data reconciliation problem significantly, even for large-scale chemical processes, (ii) is computationally simple and (iii) it conforms with the general process of variable monitoring in a chemical plant.Numerical examples are presented to clarify the elements of the procedure involved and demonstrate their value and effectiveness in dealing with realistic situations. 相似文献
106.
The kinetics of methane hydrate formation, after commencement of nucleation, were studied using a semibatch stirred tank reactor. The temperatures studied in the experiments were from 274 to 284 K over a pressure range of 3–10 MPa. The results of the experiments revealed that the formation kinetics were dependent on the interfacial area, pressure, temperature and degree of supercooling. The history of water sample affected the induction delay times for nuclei formation, but it had no observable effects on the overall kinetics of hydrate formation after the nucleation had commenced. A consistent semi-empirical model was formulated to correlate the experimental kinetic data. 相似文献
107.
Kinetic expressions used to describe the reactions of deactivating catalyst particles are applied here to the sulphation of calcined limestone in a fluidised bed coal combustor where reactivity diminishes as pores fill with sulphate. Following closely the recent work of Fieldes and Davidson it is shown how experiments with batchwise addition of limestone to the combustor may be used to derive the two reaction rate constants of the system, ks, and kd, and how these may be incorporated into a two-phase model of a fluidised bed reactor to obtain predictions of desulphurisation efficiency under conditions of continuous operation. The resulting equation for SO2 retention, η, may be simplified to:η = 1 ? [] where K is a function of limestone type and operating conditions and β is the calcium-to-sulphur mole ratio. The predictions of this equation are shown to be in agreement with experimental results. 相似文献
108.
《Expert systems with applications》2014,41(8):3726-3735
Defining appropriate pricing strategy for smart environment is important and complex task at the same time. It holds the primal fraction in Demand Response (DR) program. In our work, we devise an incentive based smart dynamic pricing scheme for consumers facilitating a multi-layered scoring rule. The proposed strategy characterizes both incentive based DR and price based DR programs facilities. This mechanism is applied between consumer agents (CA) to electricity provider agent (EP) and EP to Generation Company (GENCO). Based on the Continuous Ranked Probability Score (CRPS), a hierarchical scoring system is formed among these entities, CA–EP–GENCO. As CA receives the dynamic day-ahead pricing signal from EP, it will schedule the household appliances to lower price period and report the prediction in a form of a probability distribution function to EP. EP, in similar way reports the aggregated demand prediction to GENCO. Finally, GENCO computes the base discount after running a cost-optimization problem. GENCO will reward EP with a fraction of discount based on their prediction accuracy. EP will do the same to CA based on how truthful they were reporting their intentions on device scheduling. The method is tested on real data provided by Ontario Power Company and we show that this scheme is capable to reduce energy consumption and consumers’ payment. 相似文献
109.
The effect of an electric field on the absorption of sulfur dioxide by pure water drops is examined experimentally. Field strength is varied up to 8.0 kV/cm, and nozzle Reynolds number is varied between 26 and 78. Drop surface charge density, size, shape, shape oscillation, acceleration and total sulfur dioxide uptake are measured directly. Significant reduction in drop size and increase in acceleration with increasing field strength are the major effects observed, while alteration in drop shape and oscillation are slight. Calculated average mass transfer coefficients increase with both field strength and nozzle velocity, but total sulfur dioxide uptake decreases with field strength due to reductions in drop-gas contact time. The results suggest that the design of scrubbers with electric fields concentrated in the region of drop formation but absent elsewhere show the greatest promise for improved efficiency. 相似文献
110.
Applying the boundary element method to electrochemical calculations of primary current distribution
The computation of primary current distribution using the boundary element method has been analysed. A numerical example has been included. Values obtained numerically have been compared with those obtained experimentally. A fairly good accuracy has been observed. Some computational problems occurring when using the boundary element method for electrochemical problems have been discussed. 相似文献